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Beilstein J. Org. Chem. 2012, 8, 2118–2123, doi:10.3762/bjoc.8.238
Graphical Abstract
Scheme 1: Synthetic pathway to the desired polymer 7.
Figure 1: Cyclic voltammetry results of (A) clicked copolymer 7, (B) clicked copolymer 7 with Ad-COOK ().
Figure 2: DLS measurement of compound 2 with β-cyclodextrin (— •), alkylated polyphenol 4 (- -), product 7 (—...
Beilstein J. Org. Chem. 2011, 7, 1516–1519, doi:10.3762/bjoc.7.177
Scheme 1: Synthetic pathway to the desired β-cyclodextrin-comprising copolymer and its supramolecular system.
Figure 1: 2-D ROESY NMR spectrum of complexed β-CD with (+)-ephedrine.
Figure 2: Turbidity measurement showing different cloud points for the CD-comprising copolymer 1 (32 °C) and ...
Figure 3: DLS measurement showing hydrodynamic diameters for (a) the CD-comprising polymer and (b) for supram...
Beilstein J. Org. Chem. 2011, 7, 204–209, doi:10.3762/bjoc.7.27
Scheme 1: Synthesis of copolymers 3D, 3L and CD-complexes 4D, 4L.
Figure 1: 2D NMR ROESY spectrum of monomer 2D with RAMEB-CD.
Figure 2: 2D NMR ROESY experiment showing the correlation between protons of the phenyl moiety of 4D with the...
Figure 3: NMR shifts of the complexed monomer 2D.
Figure 4: Comparison of 1H NMR spectra of 2D and 2L complexed with β-CD.
Figure 5: Complex formation with phenolphthalein and phenylalanine as competitor.
Figure 6: Hydrodynamic diameters of the copolymers and their corresponding complexes with RAMEB-CD a) L-pheny...